Selected Methods of Structure Analysis (FSI-9VMS)

The objective is to provide the student with a sound overview of methods that are available for structural analysis (morphology, phase and local chemical composition) of metallic and non-metallic materials. In-depth knowledge will be offered about the methods that the student will employ within the experimental work necessary for the preparation of the dissertation.

In the course, which does not rely on the classical pattern of lectures but rather on consultations, the content is adapted to suit the orientation of the student's dissertation. Within the course, the student acquires the basics of all currently used methods for structure characterization (optical microscopy, transmission and scanning electron microscopy, methods of local chemical analysis in electron microscopy, scanning probe methods, X-ray structural analysis, etc.). The student will learn in depth the methods to be used while working on the dissertation.

Examination: written and oral parts

The selection of experimental methods is tailored to the focus of each doctoral student’s dissertation. The course is conducted individually through expert consultations aimed at deepening the student’s understanding and scientific interpretation of results obtained during experimental work.

Discussions may cover, in particular, the following areas:

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  Structural and phase analysis – optical and electron microscopy methods, phase identification and quantification.

  
  


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  Mechanical properties – methods for evaluating hardness, microhardness, and other parameters of mechanical behavior.

  
  


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  Analytical techniques – EDS, WDS, EBSD, EELS, XRD and their application in studying material composition and structure.

  
  


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  Data interpretation – correlation between structure, composition, and properties of materials, processing, and presentation of experimental results.